CICECO

Short CV

2016 - 2018: post-doctoral fellow at CICECO - Aveiro Institute of Materials under the supervision of Doctor Luis Mafra and Professor João Rocha;

2010 - 2016: post-doctoral fellow at CICECO - Aveiro Institute of Materials and Laboratorium für Physikalische Chemie, ETH Zürich supervised by Doctor Luis Mafra, Professor João Rocha and Professor Beat H. Meier;

2009: PhD in Physical Chemistry: " Weak intermolecular interactions in advanced functional materials: spectroscopic and computational studies” (supervision of Prof. Paulo Ribeiro-Claro), Chemistry Department, University of Aveiro. During this period, 5 months were spent in the University of Malaga, Spain, working in the group of Professor Juan Carlos Otero, developing SERS studies on pharmaceutical compounds;

2005: Degree in Physics and Chemistry (for teaching), Univ. Aveiro (17/20)

SCIENTIFIC INTERESTS

- Combining high-resolution solid-state NMR methods, X-ray diffraction and computational approaches to study crystal packing interactions in small molecules (namely pharmaceuticals) and materials - NMR crystallography;

- Study drug-drug and drug-host interactions of molecular scaffolds as drug delivery systems.

- NMR characterization of modified nanoporous solid sorbents with potential for gas capture (by using 13C-labelled CO2 in a gas mixture);

- NMR characterization of porous materials relevant in heterogeneous catalysis (study of Lewis and Brønsted acidity);

OTHER INTERESTS

- Responsible for preparing and delivering solid-state NMR Hands-on courses (II Jornadas Nacionais de Caracterização de Materiais - 2017 and IV Ibero-American NMR Meeting - 2012). - Co-President of the Young Chemists Group (GQJ) of the Portuguese Chemical Society (SPQ) between 2010-2012 - Member of the organizing committee of several scientific events: Chemistry Olympics competitions, the Portuguese Physics students meeting (2004), International conference on solubility phenomena (2004), Young Portuguese Chemists meeting (2010), European Young Chemists Network (EYCN) delegates assembly (2012) and EYCN contribution to the 4EuCheMS (2012), IV Ibero-American NMR Meeting (2012).

Scientific Interests

- NMR characterization of modified nanoporous solid sorbents with potential for gas capture (by using 13C-labelled CO2 in a gas mixture);

- NMR characterization of porous materials relevant in heterogeneous catalysis (study of Lewis and Brønsted acidity);

- Combining high-resolution solid-state NMR methods, X-ray diffraction and computational approaches to study crystal packing interactions in small molecules (namely pharmaceuticals) and materials

- NMR crystallography;

- Study drug-drug and drug-host interactions of molecular scaffolds as drug delivery systems.

Present Research Group

Dr. Luis Miguel Monteiro Mafra; Professor João Rocha; Dr. Ildefonso Marin; Dr. Marina Ilkaeva, Dr. Ricardo Vieira, Dra. Paula Soares Santos; Carlos Bornes; João Pereira

Main present collaborators

Professor Beat H. Meier (ETH - Zurich); Prof. José M. Ferreira (UA); Dr. José R.B. Gomes (UA); Prof. Isabel Neves (U. Minho); Dr. Paula Ferreira (UA); Prof. Teresa Duarte (IST); Prof. Moisés Pinto (IST); Prof. Norberto Masciocchi (U. Insubria)

Selected Publications

1. "Comparison of different silica microporous structures as drug delivery systems for in vitro models of solid tumors", Natália Vilaça, Ana F. Machado, Filipa Morais-Santos, Ricardo Amorim, A. Patrícia Neto, Enora Logodin, Manuel F. R. Pereira, Mariana Sardo, João Rocha, Pier Parpot, António M. Fonseca, Fátima Baltazar and Isabel C. Neves, RSC Adv., 2017, 7, 13104-13111.

2. "PAIN with and without PAR: Variants for third-spin assisted heteronuclear polarization transfer", Vipin Agarwal*, Mariana Sardo*, Ingo Scholz, Anja Böckmann, Matthias Ernst and Beat H. Meier, J. Biomol. NMR 2013, 56(4), 365-377. (*authors equally contributed for this work)

3. "Combining multinuclear high-resolution solid-state MAS NMR and computational methods for resonance assignment of glutathione tripeptide", Mariana Sardo, Renée Siegel, Sérgio M. Santos, João Rocha, José R. B. Gomes, Luis Mafra, J. Phys. Chem. A 2012, 116 (25), 6711–6719.

4. "3D–2D–0D Stepwise Deconstruction of a Water Framework Templated by a Nanoporous Organic–Inorganic Hybrid Host", João Rocha, Fa-Nian Shi, Filipe A. Almeida Paz, Luis Mafra, Mariana Sardo, Luis Cunha-Silva, James Chisholm, Paulo Ribeiro-Claro and Tito Trindade, Chem. Eur. J. 2010, 16, 7741-7749.

Mariana Isabel Coutinho Sardo

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New NMR Network joins 7 European and 1 American Research Centers

Short CV

Scientific Interests

Present Research Group

Main present collaborators

Selected Publications

Projects

Especies de CO2 formadas a superficie de materiais porosos para aplicacoes ambientais caracterizadas por RMN de polarizacao nuclear dinamica (GAS2MAT-DNPSENS)

PartnerFundação para a Ciência e a Tecnologia

Polymorphism in pharmaceuticals: new insights from NMR Crystallography (EXPL/QEQ-QFI/2078/2013)

CoordinatorFundação para a Ciência e a Tecnologia

Publications

Hydrogen bonding networks in gabapentin protic pharmaceutical salts: NMR and in silico studies

Unravelling the Structure of Chemisorbed CO2 Species in Mesoporous Aminosilicas: A Critical Survey

Enhancing Adamantylamine Solubility through Salt Formation: Novel Products Studied by X-ray Diffraction and Solid-State NMR

H-1-P-31 HETCOR NMR elucidates the nature of acid sites in zeolite HZSM-5 probed with trimethylphosphine oxide

Revisiting the crystal structure of dickite: X-ray diffraction, solid-state NMR, and DFT calculations study

Detecting Proton Transfer in CO2 Species Chemisorbed on Amine-Modified Mesoporous Silicas by Using (CNMR)-C-13 Chemical Shift Anisotropy and Smart Control of Amine Surface Density

Microwave-assisted N,N-dialkylation of amine-functionalized periodic mesoporous phenylene-silica: An easy and fast way to design materials

Comparison of different silica microporous structures as drug delivery systems for in vitro models of solid tumors

Packing Interactions and Physicochemical Properties of Novel Multicomponent Crystal Forms of the Anti-Inflammatory Azelaic Acid Studied by X-ray and Solid-State NMR

Interaction of CO2 and CH4 with Functionalized Periodic Mesoporous Phenylene-Silica: Periodic DFT Calculations and Gas Adsorption Measurements

Diazole-based powdered cocrystal featuring a helical hydrogen-bonded network: Structure determination from PXRD, solid-state NMR and computer modeling

X-ray and NMR Crystallography Studies of Novel Theophylline Cocrystals Prepared by Liquid Assisted Grinding

Micro- and Mesoporous Structures as Drug Delivery Carriers for Salicylic Acid

Catalytic dehydration of fructose to HMF over sulfonic acid functionalized periodic mesoporous organosilicas: role of the acid density

Monitoring hydration in lime-metakaolin composites using electrochemical impedance spectroscopy and nuclear magnetic resonance spectroscopy

Thermal and mechanical stability of lanthanide-containing glass-ceramic sealants for solid oxide fuel cells

Melilite glass-ceramic sealants for solid oxide fuel cells: effects of ZrO2 additions assessed by microscopy, diffraction and solid-state NMR

Potentiation of 5-fluorouracil encapsulated in zeolites as drug delivery systems for in vitro models of colorectal carcinoma

PAIN with and without PAR: variants for third-spin assisted heteronuclear polarization transfer

Combining Multinuclear High-Resolution Solid-State MAS NMR and Computational Methods for Resonance Assignment of Glutathione Tripeptide

Zeolite Structures Loading with an Anticancer Compound As Drug Delivery Systems

3D-2D-0D Stepwise Deconstruction of a Water Framework Templated by a Nanoporous Organic-Inorganic Hybrid Host

Inclusion compounds of phenol derivatives with cyclodextrins: a combined spectroscopic and thermal analysis

Hydrogen bonding in nitrofurantoin polymorphs: a computation-assisted spectroscopic study

The solid-liquid phase diagrams of binary mixtures of consecutive, even saturated fatty acids: differing by four carbon atoms

The solid-liquid phase diagrams of binary mixtures of consecutive, even saturated fatty acids

Surface-enhanced Raman scattering of 5-fluorouracil adsorbed on silver nanostructures

Pseudopolymorphic transitions of niclosamide monitored by Raman spectroscopy

Surface enhanced Raman scattering of trans-3-hydroxycinnamic acid adsorbed on silver nanoparticles

Characterisation of pharmaceutical solids combining NMR, X-ray diffraction and computer modelling

Calculation of NMR tensors: application to small molecule pharmaceutics

Solid-state NMR applications in the structural elucidation of small molecules

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